Analytical Instrumentation & Environmental Monitoring


Accurate humidity measurements under extreme conditions

November 2002 Analytical Instrumentation & Environmental Monitoring

Manufacturers Testo GmbH of Germany and Coresci in France have developed new sensors that make humidity measurements under extreme conditions possible with increased accuracy and reliability. Measurement methods like hair hygrometers, psychrometers (temperature probe covered with a damp cotton sock) and dew point mirrors (a mirror cooled down until condensation shows) are fast being replaced by electronic instruments.

The conventional methods have proved to be either inaccurate, too cumbersome and operator intensive or not robust enough. None permitted measurements at high temperatures. Best accuracy seldom exceeded 2% relative humidity (RH), even when using a psychrometer with high precision RTDs. Then these results still had to be interpreted by means of cumbersome charts like the Mollier diagram.

Traditional RH measurement methods are being replaced by fast, robust, solid-state electronic instruments
Traditional RH measurement methods are being replaced by fast, robust, solid-state electronic instruments

Small and robust

With the development of the capacitive sensor, compact and portable instrumentation has been made possible. Sensors for fixed process applications are essentially similar in size to a temperature sensor. Different shapes of capacitive humidity sensors now allow measurement within products - for example, their design permits the insertion of flat humidity probes (5 mm) into rolls of textiles, between stacks of paper or carton - and special sintered filters allow the use of probes within dusty bulk materials like grain, polymers, powders, etc.

Measuring extremes

Testo and Coresci (which is now part of Gefran in Italy) provide sensors that allow measurement of 0 to full 100% RH - this means that the modern sensor can survive even being dipped in water.

Long-term tests around the world (since 1996 a set of sensors from Testo have been tested at the PTB, CETIAT, NIST, IMGC, NPL and INTA) under adverse conditions show that the accuracy of Testo's new capacitive sensor remains within 1% RH consistently. This level of accuracy, sensor stability and measurement reproducibility was hitherto impossible.

Sensors for special applications

Humidity sensors now operate up to process temperatures of 180°C with 1% RH accuracy. Relative humidity probes can be supplied for operation under high pressures - up to 5 MPa (50 bar). This makes the measurement (and therefore the control) of efficiency of refrigeration and adsorption dryers possible. Pressure dewpoints down to -60° Ctpd can be measured using Testo's new FA-200 dewpoint measuring instrument.

Online calibration and checking using the model 650 reference instrument allows the user to perform ISO 9000 checks regularly. (This instrument also performs all required calculations for which the expert required the Mollier diagram in the past.)

Humidity generator and reference probe

For calibration laboratories, Testo supplies complete humidity generators equipped with Testo's 1% RH humidity reference probe and reference instrument 650. All instruments and probes are available with ISO or DKD calibration certification.

Water activity measurement (aw) made easy

Within the pharmaceutical, chemical and food industries the measurements of a product's water activity value (aw) are becoming increasingly important.

The aw value is a direct indication of the product's hygro interaction with the surrounding air - whether the product will absorb moisture or release it when exposed to air. The measurement is gaining importance with regard to the stringent HACCP regulations as aw is indicative of bacterial and fungal growth conditions. The Testo 650 water activity chamber is equipped with a fast humidity reference probe and within a few minutes the aw value for any material or product can be determined without elaborate procedures or equipment.

Selecting the correct sensors and probes

Criteria for selection vary for different applications and should include:

* Accuracy.

* Stability and reproduceability.

* Temperature requirements.

* Ambient conditions.

* Robustness.

UniTemp, the importers of both the Testo and Gefran (Coresci) range of products, offer a wide selection of process humidity transmitters as well as portable sensors and instruments. These include cost-effective sensors for climate control in building and agricultural applications and general industrial measurements as well as the laboratory type reference probes and instruments. Filters to protect against dust and particles are selected according to application. Calibration kits and humidity generators also form part of this product range.

The humidity sensors used in many probes and transmitters are replaceable for ease of maintenance. For OEMs, UniTemp also offers the Coresci capacitive humidity sensor elements.

For more information contact UniTemp, 021 762 8995, [email protected]





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